Forschungsbericht 2011



Visualization of Carbon Nanotubes in Polymer Composites

Institut: E-12
Projektleitung: Wolfgang Bauhofer
Stellvertretende Projektleitung: Wolfgang Bauhofer
Mitarbeiter/innen: Wenjing Li
Laufzeit: 01.10.2009 — 30.09.2012
Finanzierung:Deutsche Forschungsgemeinschaft (DFG)

Introduction

Visualization of embedded carbon nanotubes (CNTs) in polymer nanocomposites using a scanning electron microscope (SEM) is shown to be a convenient and effective technique to evaluate CNT dispersion. However, the visibility of CNTs in a polymeric matrix is sensitive to many factors, such as the concentration and distribution of the CNTs, observation parameters, including accelerating voltage, current of primary electrons and scanning speed. Understanding these influencing factors provides helpful information for material scientists for obtaining SEM images of high quality.

 

Major goals the project:

  • Investigating the influencing parameters on CNT visibility.
  • Understanding the image mechanism.
  • Evaluating image depth.

Recent SEM observation of CNT/epoxy composites prepared by stirring and calendering shows a good CNT dispersion in epoxy matrix favors the visibility of CNTs, and the CNTs exhibit improved bright contrast with increasing accelerating voltage.

Wissenschaftliche Kontakte und Kooperationen

  • Prof. Dr. Hans-Joachim Fitting, Institute of Physics, University of Rostock

Introduction

Visualization of embedded carbon nanotubes (CNTs) in polymer nanocomposites using a scanning electron microscope (SEM) is shown to be a convenient and effective technique to evaluate CNT dispersion. However, the visibility of CNTs in a polymeric matrix is sensitive to many factors, such as the concentration and distribution of the CNTs, observation parameters, including accelerating voltage, current of primary electrons and scanning speed. Understanding these influencing factors provides helpful information for material scientists for obtaining SEM images of high quality.

 

Major goals the project:

  • Investigating the influencing parameters on CNT visibility.
  • Understanding the image mechanism.
  • Evaluating image depth.

Recent SEM observation of CNT/epoxy composites prepared by stirring and calendering shows a good CNT dispersion in epoxy matrix favors the visibility of CNTs, and the CNTs exhibit improved bright contrast with increasing accelerating voltage.

Wissenschaftliche Kontakte und Kooperationen

  • Prof. Dr. Hans-Joachim Fitting, Institute of Physics, University of Rostock

Stichworte

  • Carbon nanotube
  • Scanning electron microscope
  • Visibility
  • Voltage contrast

Publikationen

  • Li, W., and Bauhofer, W.: Imaging of CNTs in a polymer matrix at low accelerating voltages using a SEM Carbon, vol. 49(no. 12): S. pp. 3891–3898, May 2011.
  • Li, W., Zhou, Y., Fitting, H.-J., and Bauhofer, W.: Imaging mechanism of carbon nanotubes on insulating and conductive substrates using a scanning electron microscope Journal of Materials Science, vol. 46(no. 23): S. pp. 7626–7632, July 2011.
  • Li, W., Buschhorn, S.T., Schulte, K., and Bauhofer, W.: The imaging mechanism, imaging depth, and parameters influencing the visibility of carbon nanotubes in a polymer matrix using an SEM Carbon, vol. 49(no. 6): S. pp. 1955–1964, January 2011.